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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 2
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Original Articles

Efficient Synthesis of 4-Methyl-L,10-Phenanthroline Starting from 8-Aminolepidine

Stephane Lutun Laboratoire de Chimie Organique et Environnement, Bat. C4 - Université des Sciences et Technologies de Lille, 59655, Villeneuve d'Ascq Cedex, France
,
Eric Guichard Laboratoire de Chimie Organique et Environnement, Bat. C4 - Université des Sciences et Technologies de Lille, 59655, Villeneuve d'Ascq Cedex, France
,
Bruno Hasiak Laboratoire de Chimie Organique et Environnement, Bat. C4 - Université des Sciences et Technologies de Lille, 59655, Villeneuve d'Ascq Cedex, France
&
Daniel Couturier Laboratoire de Chimie Organique et Environnement, Bat. C4 - Université des Sciences et Technologies de Lille, 59655, Villeneuve d'Ascq Cedex, France
Pages 175-180 | Accepted 25 Apr 1998, Published online: 17 Sep 2007
 
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Abstract

8-aminolepidine 2 reacted with glycerol 3 in presence of sodium iodide and gave 4-methyl-l,10-phenanthroline 1 with a 66 % yield.

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