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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 4
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Original Articles

Mild Synthesis of α-Oxoketene O.N-Acetals from β-Oxothioxo Esters and Amines

Isao Furukawa Department of Molecular Science and Technology, Faculty of Engineering, Doshisha University, Kyotanabe, Kyoto, 610-0394, Japan
,
Hironori Fujisawa Department of Molecular Science and Technology, Faculty of Engineering, Doshisha University, Kyotanabe, Kyoto, 610-0394, Japan
,
Tetsuji Abe Department of Molecular Science and Technology, Faculty of Engineering, Doshisha University, Kyotanabe, Kyoto, 610-0394, Japan
&
Tetsuo Ohta Department of Molecular Science and Technology, Faculty of Engineering, Doshisha University, Kyotanabe, Kyoto, 610-0394, Japan
Pages 599-606 | Received 02 Jul 1998, Published online: 17 Sep 2007
 
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Abstract

α-Oxoketene O,N-acetals were prepared from β-oxothiono esters and primary amines in the presence of triethylamine at room temperature within several hours in good yields.

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