Synthesis of Hydroxycedranone and Aminohydroxycedrane

Yilin Song Department of Chemistry, Fudan University, Shanghai, 200433, P. R. China

Quanrui Wang Department of Chemistry, Fudan University, Shanghai, 200433, P. R. China

Zongbiao Ding Department of Chemistry, Fudan University, Shanghai, 200433, P. R. China

Fenggang Tao Department of Chemistry, Fudan University, Shanghai, 200433, P. R. China

Abstract

Two optically pure derivatives of α-cedrene — (1R,2R,5S,7R,8R)- 8-hydroxy-9-cedranone 2 and (lR,2R,5S,7R,8R,9S)-9-amino-8-hydroxycedrane 4 were prepared conveniently. An X-ray structural analysis of 2 was performed indicating that the hydroxycedranone exists as dimer due to one hydrogen bond in solid state.

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Synthesis of Hydroxycedranone and Aminohydroxycedrane

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Synthesis of Hydroxycedranone and Aminohydroxycedrane

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