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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 22
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Original Articles

Studies on Calix(aza)crqwns, III. Synthesis of 1,3-Alternate Calix[4]arenes Capped by Diamide Bridges

István Bitter Department of Organic Chemical Technology, Technical University of Budapest, H-1521, Budapest, Hungary
,
Alajos Grün Department of Organic Chemical Technology, Technical University of Budapest, H-1521, Budapest, Hungary
,
Barbara Balázs Technical Analytical Research Group of the Hungarian Academy of Sciences, Institute for General and Analytical Chemistry of the Technical University of Budapest, H-1521, Budapest, Hungary
,
Gábor Tóth Technical Analytical Research Group of the Hungarian Academy of Sciences, Institute for General and Analytical Chemistry of the Technical University of Budapest, H-1521, Budapest, Hungary
,
Gyula Horváth Institute for Drug Research, H-1325, Budapest, Hungary
&
László Töke Department of Organic Chemical Technology, Technical University of Budapest, H-1521, Budapest, Hungary
Pages 3905-3917 | Accepted 19 Mar 1999, Published online: 17 Sep 2007
 
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Abstract

The akylation of calix[4]arenes 1 capped by diamide bridges gave fully substituted compounds 5 and 6 of 1,3-alternate conformation. Diesters 6 were cyclized with diamines to afford doubly capped derivatives 7.

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