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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 22
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Original Articles

A Simple and Efficient Procedure for the Preparation of Benzal Chlorides and Benzal Bromides

Eric Lénel Laboratoire d'Electrochimie, Catalyse et Synthése Organique (UMR7582), C.N.R.S.-Université Paris 12 Val de Marne, 2, Rue H. Dunant 94320, Thiais, France
,
Jean-Paul Paugam Laboratoire d'Electrochimie, Catalyse et Synthése Organique (UMR7582), C.N.R.S.-Université Paris 12 Val de Marne, 2, Rue H. Dunant 94320, Thiais, France
,
Monique Heintz Laboratoire d'Electrochimie, Catalyse et Synthése Organique (UMR7582), C.N.R.S.-Université Paris 12 Val de Marne, 2, Rue H. Dunant 94320, Thiais, France
&
Jean-Yves Nédélec Laboratoire d'Electrochimie, Catalyse et Synthése Organique (UMR7582), C.N.R.S.-Université Paris 12 Val de Marne, 2, Rue H. Dunant 94320, Thiais, France
Pages 4015-4024 | Received 01 Dec 1998, Published online: 17 Sep 2007
 
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Abstract

Benzal chlorides and benzal bromides were conveniently synthesized by reaction of aryl aldehydes with a Vilsmeier type reagent formed in situ by reduction of CC14 or CBr4 in dimethylformamide (DMF) as solvent.

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