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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 22
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Original Articles

Synthesis of 1-Bromo-3-buten-2-one

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Pages 4035-4042 | Accepted 06 Jan 1999, Published online: 17 Sep 2007
 

Abstract

A synthetic method for 1-bromo-3-buten-2-one is given. The compound is prepared through the following sequence: 2-butanone to 2-methyl-2-ethyl-1,3-dioxolane to 2-(1-bromoethyl)-2-bromomethyl-1,3-dioxolane to 2-bromomethyl-2-vinyl-1,3-dioxolane to the final product. Full experimental details including spectral data are given.

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