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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 20
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Original Articles

Preparation of 1,1,3,-Tetraisopropyl-l,3-Dichlorodisiloxane and Triisopropylchlorosilane

Ram Chawla Sivento Inc. 2 Turner Place, Piscataway, NJ, 08855
&
Gerald L. Larson Sivento Inc. 2 Turner Place, Piscataway, NJ, 08855
Pages 3499-3501 | Received 18 Mar 1999, Published online: 17 Sep 2007
 
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Abstract

A facile, hydrochloric acid-free chlorination of silanes was developed. This allows for the elimination of siloxane bond cleavage and chlorination of carbon-hydrogen bonds during the chlorination of the Si-H bond.

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