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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 20
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Original Articles

An Efficient Synthesis of N-Trifluoroacetyl Adriamycin-14-Valerate (AD-32)

Cheng Ma Department of Chemistry, Zhejiang University, Hangzhou, 310027, P.R.China
,
Yan-Guang Wang Department of Chemistry, Zhejiang University, Hangzhou, 310027, P.R.China
,
Jian-Feng Shi Department of Chemistry, Zhejiang University, Hangzhou, 310027, P.R.China
,
Yao-Zu Chen Department of Chemistry, Zhejiang University, Hangzhou, 310027, P.R.China
&
Yun-Hua Chen Zhejiang HISUN Pharmaceutical Co., LTD, Taizhou, 318000, P.R.China
Pages 3581-3586 | Received 01 Feb 1999, Published online: 17 Sep 2007
 
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Abstract

An eficent, one-pot procedure is reported for the synthesis of N-trifluoroacetyl adriamycin-14-valerate (AD-32, 3) from daunorubicin (1) in 35% overall yield.

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