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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 21
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Original Articles

Reaction of bis(Sym-Collidine)-Bromine(I) Hexafluorophosphate with α-Diazo Esters

Gérard Rousseau Laboratoire des Carbocycles (AsSocié au CNRS), Institut de Chimie Moléculaire d'Orsay, B[acaron]t. 420, Université de Paris-Sud, 91405, Orsay, France E-mail: [email protected]
&
Jean-Xavier Marie Laboratoire des Carbocycles (AsSocié au CNRS), Institut de Chimie Moléculaire d'Orsay, B[acaron]t. 420, Université de Paris-Sud, 91405, Orsay, France E-mail: [email protected]
Pages 3705-3710 | Accepted 28 Feb 1999, Published online: 17 Sep 2007
 
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Abstract

Reaction of α-diazo esters with bis(sym-collidine)bromine(I) hexafluorophosphate in methylene chloride at -40°C led to a-bromo-α, β-unsaturated esters.

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