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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 21
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Original Articles

One Step and Convenient Preparations of 4-Hydroxyretinal and 4-Oxoretinal

Masaru Hashimoto Faculty of Agriculture and Life Science, Hirosaki University, 3 Bunkyo-cho, Hirosaki, 036-8561, Japan; Department of Chemistry, Columbia University, New York, New York, 10027
&
Yukari Fujimoto Department of Chemistry, Columbia University, New York, New York, 10027
Pages 3793-3797 | Received 06 Apr 1999, Published online: 17 Sep 2007
 
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Abstract

Treatment of all-trans-retinal with one and two equivalents of NBS in a mixture of CH3CN-CH2Cl2-H2O provide 4-hydroxyretinal and 4-oxoretinal, respectively, in good yields.

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