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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 6
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Original Articles

Efficient and Chemoselective N-Nitrosation of Secondary Amines Under Mild and Heterogeneous Conditions with Sodium Nitrite and Oxalic Acid Two Hydrate

Mohammad Ali Zolfigol Chemistry Department, College of Science, Bu-Ali Sina University, Hamadan, 65174, Iran
Pages 905-910 | Accepted 19 Aug 1998, Published online: 17 Sep 2007
 
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Abstract

Secondary amines can be quantitatively converted to their corresponding nitroso derivatives with a combination of oxalic acid and sodium nitrite in dichloromethane at room temperature.

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