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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 7
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Original Articles

Microwave Thermolysis Vi : A Rapid and General Method for Dethioacetalization Using “Clayan” in Dry Media

H. M. Meshram Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
Gondi Sudershan Reddy Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
G. Sumitra Indian Institute of Chemical Technology, Hyderabad, 500 007, India
&
J. S. Yadav Indian Institute of Chemical Technology, Hyderabad, 500 007, India
Pages 1113-1119 | Received 23 Sep 1998, Published online: 17 Sep 2007
 
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Abstract

A variety of thioacetals, dithiolanes and dithianes are deprotected into their carbonyl compounds using clay supported ammonium nitrate “Clayan” under microwave irradiation. The present method avoids the use of toxic oxidants and excess of solvent.

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