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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 8
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Original Articles

Stereoselective Borane Reduction of Acetophenone using 1,3,2-Oxazaborolidine Derived from (R)-4-(Diphenylhydroxymethyl)-1,3-Thiazolidine

Monique Calmes Laboratoire des Aminoacides, Peptiees et Protéines, UMR 5810 Universités Montpellier I et II, UMII, Place E. Bataillon, 34095, Montpellier cedex 5, France
&
Francoise Escale Laboratoire des Aminoacides, Peptiees et Protéines, UMR 5810 Universités Montpellier I et II, UMII, Place E. Bataillon, 34095, Montpellier cedex 5, France
Pages 1341-1347 | Received 06 Oct 1998, Published online: 17 Sep 2007
 
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Abstract

A new chiral 1, 3, 2-oxazaborolidine derived from (R)-4-(diphenylhydroxymethyl)-l, 3-thiazolidine has been synthesized and its efficiency in the asymmetric reduction of acetophenone by borane has been investigated. It gives (R)-l-phenylethanol with high enantiomeric excess

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