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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 8
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Original Articles

Synthesis of Ocimin, A 1,5-Diene, by a Bis- Grignard Reaction

Martha A. Ornelas Facultad de Ciencias Quíicas, Universidad Autónoma de Baja California, C.P. 22390, Otay Universidad, Tijuana, B.C., Mexico
,
Raul Romero Facultad de Ciencias Quíicas, Universidad Autónoma de Baja California, C.P. 22390, Otay Universidad, Tijuana, B.C., Mexico
&
Ratnasamy Somanathan Centra de Graduados e Investigacion del Instituto Tecnologico de Tijuana, Apto. Postal 1166, C.P. 22000, Tijuana, B.C., Mexico
Pages 1401-1403 | Received 13 Oct 1998, Published online: 17 Sep 2007
 
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Abstract

Ocimin, 1,6-bis-(4-methoxyphenyl)-(E)-(E)-hexa- 1,5-diene, was synthetized by the bis-Grignard reaction of p-anisaldehyde with 1,4-bis- (br0momagnesium)butane and the dehydration of the intermediate diol using triphenylphosphine-carbon tetrachloride.

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