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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 9
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Original Articles

Synthesis Of Diacetals By Condensation Of Carbonyl Compounds With Bis(Hydrox Ymethyl)-1,3-Propanediol Catalysed By Expansive Graphite

Tong-Shou Jin Department of Chemistry, Hebei University, Baoding, 071002, P.R., China
,
Tong-Shuang Li Department of Chemistry, Hebei University, Baoding, 071002, P.R., China
,
Zhan-Hui Zhang Department of Chemistry, Hebei University, Baoding, 071002, P.R., China; Department of Chemistry, Hebei Teachers' University, Shijiazhuang 050091, Hebei Province, P.R., China
&
Yan-Jun Yuan Department of Chemistry, Hebei University, Baoding, 071002, P.R., China
Pages 1601-1606 | Accepted 19 Sep 1998, Published online: 17 Sep 2007
 
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Abstract

Synthesis of diacetals from 2,2-bis(hydroxymethyl)-1,3-propanediol with aldehydes and ketones under catalysis of expansive graphite in refluxing benzene or toluene in good to excellent yield has been described.

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