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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 15
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Original Articles

An Expedient Synthesis of Allylic Polyprenyl Phosphates

Clive L. Branch Department of Medicinal Chemistry, SmithKline Beecham Pharmaceuticals, New Frontiers Science Park (North), Third Avenue, Harlow, Essex, England, CM19 5AW
,
George Burton Department of Medicinal Chemistry, SmithKline Beecham Pharmaceuticals, New Frontiers Science Park (North), Third Avenue, Harlow, Essex, England, CM19 5AW; Dept. Medicinal Chemistry, SB Pharmaceuticals, R&D, 1250 South Collegeville Road, PO Box 5089, Collegeville, PA, 19426, USA
&
Stephen F. Moss Department of Medicinal Chemistry, SmithKline Beecham Pharmaceuticals, New Frontiers Science Park (North), Third Avenue, Harlow, Essex, England, CM19 5AW
Pages 2639-2644 | Received 08 Jul 1998, Published online: 25 Sep 2007
 
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Abstract

Allylic polyprenyl phosphates 6c-d have been prepared in high yield from polyprenyl alcohols via an operationally straightforward oxidation and deprotection sequence utilising phosphite triesters 4.

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