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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 24
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Original Articles

Oxidation of Enolate Anion by Hypervalent Iodine Compounds: Synthesis of α-Tempo Carbonyl Compound, A New Living Radical Polymerization Initiator

Kwang-Hyun AhnDepartment of Chemistry, Kyung Hee University, Yongin City, 449-701, Korea
&
Younghun KimDepartment of Chemistry, Kyung Hee University, Yongin City, 449-701, Korea
Pages 4361-4366 | Received 22 Feb 1999, Published online: 25 Sep 2007
 
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Abstract

Oxyfunctionalization of esters, 1, by (diacetoxyiodo)benzene and 2,2,6,6-tetramethylpiperidinyl-l-oxy radical produced α-TEMPO esters, 2, which are an efficient unimolecular initiator for the living radical polymerization.

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