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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 2
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Original Articles

NITRATION OF AROMATIC COMPOUNDS ON SOLID CATALYSTS

Tomasz Miłczak Division of Highenergetic Materials, Faculty of Chemistry, Warsaw University of Technology (Politechnika), Noakowskiego, 3, Warszawa, 00-664, Poland
,
Jarosław Jacniacki Division of Highenergetic Materials, Faculty of Chemistry, Warsaw University of Technology (Politechnika), Noakowskiego, 3, Warszawa, 00-664, Poland
,
Janusz Zawadzki Division of Highenergetic Materials, Faculty of Chemistry, Warsaw University of Technology (Politechnika), Noakowskiego, 3, Warszawa, 00-664, Poland
,
Monika Malesa Division of Highenergetic Materials, Faculty of Chemistry, Warsaw University of Technology (Politechnika), Noakowskiego, 3, Warszawa, 00-664, Poland
&
Wincenty Skupiński Division of Highenergetic Materials, Faculty of Chemistry, Warsaw University of Technology (Politechnika), Noakowskiego, 3, Warszawa, 00-664, Poland
Pages 173-187 | Published online: 16 Aug 2006
 
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Abstract

o-Xylene, phenol and toluene were nitrated with 100% nitric acid on MoO3/SiO2, WO3/SiO2, TiO2/SiO2, and TiO2–WO3/SiO2 systems. Phenol and toluene were nitrated with yields higher than 90%, and the 10% and 15% MoO3/SiO2 catalysts were most active in the nitration of o-xylene. The most active catalysts exhibited the para-position selectivity of nitration.

Acknowledgments

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