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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 11
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Original Articles

A RAPID AND EFFICIENT METHOD OF THIOACETALIZATION OF CARBONYL COMPOUNDS CATALYSED BY POCl3-MONTMORILLNITE

Tong-Shou Jin Department of Chemistry, Hebei University, Baoding, 071002, P.R. ChinaCorrespondence[email protected]
,
Xu Sun Department of Chemistry, Hebei University, Baoding, 071002, P.R. China
,
Yan-Ran Ma Department of Chemistry, Hebei University, Baoding, 071002, P.R. China
&
Tong-Shuang Li Department of Chemistry, Hebei University, Baoding, 071002, P.R. China
Pages 1669-1673 | Accepted 03 Aug 2000, Published online: 09 Nov 2006
 
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Abstract

Aldehydes and ketones were thioactalized with 1,2- ethanedithiol in the presence POCl3-montmorillonite at room temperature in excellent yields.

ACKNOWLEDGMENTS

The project was supported by NSFC (29872011), Education Committee of China and Education Committee of Hebei Province (99014).

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