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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 8
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Original Articles

OXIDATION OF URAZOLES UNDER MILD AND HETEROGENEOUS CONDITIONS WITH KHSO5 AND NaNO2

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Pages 1149-1154 | Received 26 Apr 2000, Published online: 09 Nov 2006
 

Abstract

A combination of potassium monopersulfate and sodium nitrite in the presence of wet SiO2 was used as an effective oxidizing agent for the oxidation of urazoles and bis-urazoles to their corresponding triazolinediones under mild and heterogeneous conditions with excellent yields.

ACKNOWLEDGMENTS

Financial support for this work by the Research Affairs of Bu-Ali Sina University, Hamadan, Iran, is gratefully acknowledged.

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