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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 8
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Original Articles

N-NITROSATION OF SECONDARY AMINES UNDER MILD AND HETEROGENEOUS CONDITIONS

Mohammad Ali Zolfigol Chemistry Department, College of Science, Bu-Ali Sina University, Hamadan, 65174, IranCorrespondence[email protected]
,
Mojtaba Bagherzadeh Chemistry Department, College of Science, Bu-Ali Sina University, Hamadan, 65174, Iran
,
Arash Ghorbani Choghamarani Chemistry Department, College of Science, Bu-Ali Sina University, Hamadan, 65174, Iran
,
Hassan Keypour Chemistry Department, College of Science, Bu-Ali Sina University, Hamadan, 65174, Iran
&
Sadegh Salehzadeh Chemistry Department, College of Science, Bu-Ali Sina University, Hamadan, 65174, Iran
Pages 1161-1166 | Received 26 Apr 2000, Published online: 09 Nov 2006
 
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Abstract

A combination of potassium monopersulfate and sodium nitrite in the presence of wet SiO2 was used as an effective nitrosating agent for the nitrosation of secondary amines to their corresponding nitroso derivatives under mild and heterogeneous conditions in excellent yields.

ACKNOWLEDGMENTS

Financial support for this work by the Research Affairs of Bu-Ali Sina University, Hamadan, Iran, is gratefully acknowledged.

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