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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 18
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Original Articles

SYNTHESIS OF SOLID-PHASE BOUND SULFONATE ESTERS

, , , &
Pages 2795-2802 | Received 28 Nov 2000, Published online: 15 Aug 2006
 

Abstract

p-Pivaloyloxybenzenesulfonyl and methylsulfonyl residues were used as linkers to attach secondary alcohols to Wang resin and to Merrifield resin, respectively. p-Pivaloyloxybenzenesulfonates of alcohols were deprotected at the phenolic group and coupled with Wang resin by Mitsunobu reaction whereas mesylates were lithiated at the methyl group and subsequently connected with chloromethyl residues of Merrifield resin.

ACKNOWLEDGMENT

This work was supported by the State Committee for Research Grant No. T 09/PBZ.6.04

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