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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 19
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Original Articles

PREPARATION OF TRIBUTYLBORANE FROM BUTYLLITHIUM AND BORON TRIFLUORIDE ETHERATE

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Pages 2939-2942 | Received 19 Sep 2000, Published online: 16 Aug 2006
 

Abstract

A convenient laboratory synthesis of tributylborane from commercially available n-butyllithium and boron trifluoride etherate is developed.

ACKNOWLEDGMENTS

The authors gratefully acknowledge the financial supports from the Chinese Academy of Sciences (CAS “Knowledge Innovation” Project), the Life Science Special Fund of CAS Supported by the Ministry of Finance (Stz 98-3-03), The Major State Basic Research Development Program (G2000077502), the Ministry of Science and Technology of China (970211006-06), and the National Natural Science Foundation of China (29832020, 20025207).

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