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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 2
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Original Articles

A Selective Conversion of Sulfides to Sulfoxides in 3-Fluorophenol

Wei Liang Xu School of Chemical Engineering and Environment, Beijing Institute of Technology, No. 5, Zhang Guan Cun South Avenue, Hai Dian District, Beijing, 100081, P.R. ChinaCorrespondence[email protected]
,
Yun Zheng Li School of Chemical Engineering and Environment, Beijing Institute of Technology, No. 5, Zhang Guan Cun South Avenue, Hai Dian District, Beijing, 100081, P.R. China
,
Qing Shan Zhang School of Chemical Engineering and Environment, Beijing Institute of Technology, No. 5, Zhang Guan Cun South Avenue, Hai Dian District, Beijing, 100081, P.R. China
&
He Sun Zhu School of Chemical Engineering and Environment, Beijing Institute of Technology, No. 5, Zhang Guan Cun South Avenue, Hai Dian District, Beijing, 100081, P.R. China
Pages 231-237 | Received 27 May 2003, Published online: 18 Oct 2011
 
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Abstract

A novel, convenient and selective procedure of oxidizing sulfides to sulfoxides with 30% aqueous H2O2 in 3-fluorophenol at room temperature was described. The procedure was very simple and no strict conditions were required for the selective conversion. The reaction was finished within 20 min and the yield was excellent. The specific role of the solvent in the selectivity was also exhibited.

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