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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 7
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Original Articles

A Novel Reaction of Aldeoxime with Dimedone Under Microwave Irradiation

Shujang Tu Department of Chemistry, Key Laboratory of Biotechnology on Medical Plant, Xuzhou Normal University, Jiangsu, Xuzhou, Jiangsu, 221009, P.R. ChinaCorrespondence[email protected]
,
Yuan Gao Department of Chemistry, Shenzhen University, Shenzhen, Guangdong, P.R. China
,
Chunbao Miao Department of Chemistry, Key Laboratory of Biotechnology on Medical Plant, Xuzhou Normal University, Jiangsu, Xuzhou, Jiangsu, 221009, P.R. China
,
Tuanjie Li Department of Chemistry, Key Laboratory of Biotechnology on Medical Plant, Xuzhou Normal University, Jiangsu, Xuzhou, Jiangsu, 221009, P.R. China
,
Xiaojing Zhang Department of Chemistry, Key Laboratory of Biotechnology on Medical Plant, Xuzhou Normal University, Jiangsu, Xuzhou, Jiangsu, 221009, P.R. China
,
Songlei Zhu Department of Chemistry, Key Laboratory of Biotechnology on Medical Plant, Xuzhou Normal University, Jiangsu, Xuzhou, Jiangsu, 221009, P.R. China
,
Fang Fang Department of Chemistry, Key Laboratory of Biotechnology on Medical Plant, Xuzhou Normal University, Jiangsu, Xuzhou, Jiangsu, 221009, P.R. China
&
Daqing Shi Department of Chemistry, Key Laboratory of Biotechnology on Medical Plant, Xuzhou Normal University, Jiangsu, Xuzhou, Jiangsu, 221009, P.R. China
 show all
Pages 1289-1294 | Received 28 Jul 2003, Published online: 21 Aug 2006
 
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Abstract

The reaction of aldeoxime with dimedone and ammonium acetate in glycol under microwave irradiation has been carried out, elimination and cyclization happened and acridine derivatives were obtained. The structure of the product has been thoroughly studied by x‐ray crystallographic analysis.

Acknowledgments

We thank the Nature Science Foundation of the Jiangsu Province (No. BK2001142) and the Nature Science Foundation of Jiangsu Education Department (No. 01KJB150008) and the Key Laboratory of Chemical Engineering and Technology of the Jiangsu Province Open Foundation (No. KJS02060) for financial support.

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