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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 8
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Original Articles

O‐Acylation of 3‐Methylpyrazol‐5‐ones with Acylisothiocyanates

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Pages 1507-1513 | Received 26 Jun 2003, Published online: 21 Aug 2006
 

Abstract

3‐Methylpyrazol‐5‐ones 1 react by the O‐acylation pattern with acylisothiocyanates 2 in the solvent mixture ethanol–dioxane in the presence of the equimolar amount of potassium hydroxide to produce 5‐acyloxy‐3‐methyl‐1H‐pyrazoles 3.

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