Preparation of Alkyl Nitrates, Nitrites, and Thiocyanates from Alcohols Utilizing Trichloroisocyanuric Acid with Triphenylphosphine

Gene A. Hiegel Department of Chemistry and Biochemistry, California State University, Fullerton, Fullerton, California, 92834, USACorrespondence[email protected]

Jeremiah Nguyen Department of Chemistry and Biochemistry, California State University, Fullerton, Fullerton, California, 92834, USA

Yan Zhou Department of Chemistry and Biochemistry, California State University, Fullerton, Fullerton, California, 92834, USA

Abstract

Alcohols in acetonitrile are converted into alkyl nitrates, nitrites, or thiocyanates by the action of triphenylphosphine and trichloroisocyanuric acid along with silver nitrate, silver nitrite, or sodium thiocyanate, respectively.

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Acknowledgment

This research was supported in part by an award from Rohm and Haas Company: Otto Haas Award for Technical Excellence (courtesy of Robert K. Barr).

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Preparation of Alkyl Nitrates, Nitrites, and Thiocyanates from Alcohols Utilizing Trichloroisocyanuric Acid with Triphenylphosphine

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Preparation of Alkyl Nitrates, Nitrites, and Thiocyanates from Alcohols Utilizing Trichloroisocyanuric Acid with Triphenylphosphine

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