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Original Article

Debonding-on-demand Fe3O4-epoxy adhesively bonded dissimilar joints via electromagnetic induction heating

, , , , &
Pages 734-764 | Received 23 May 2023, Accepted 04 Sep 2023, Published online: 13 Sep 2023
 

ABSTRACT

We investigated the debonding on-demand (DoD) of adhesively bonded hybrid dissimilar joints by applying electromagnetic induction heating to the joint overlap section, wherein the epoxy resin is reinforced with iron oxide (Fe3O4) particles. Ti-6Al-4 V adherends were bonded with CFRP or GFRP adherends using neat/modified epoxy adhesive. DoD tests revealed that eddy current heating of Ti-6Al-4 V was a dominant heating mechanism of the joints while both eddy current and magnetic hysteresis of CFRP and Fe3O4 acted as a secondary heating factor. A low content Fe3O4 and thinner composite adherend reduced the time to failure of the joints. Likewise, CFRP required a shorter time for debonding compared to GFRP due to its electromagnetic properties. Modifications with 2 and 5 wt.% Fe3O4 for CFRP and GFRP joints led to 31% and 37% time reduction which will be crucial for energy-saving when debonding large structures. Remarkably, sandblasting improved the electromagnetic induction capabilities of Ti-6Al-4 V, leading to a notable increase in the heating rate, which jumped from around 20°C/s to 80°C/s. Sandblasting enhanced the surface roughness of the adherends but only the water contact angle of GFRP decreased considerably. Fe3O4 modifications increased the epoxy residue on the Ti-6Al-4 V surface from 26% to 99%. DIC revealed the strain distribution of bulk materials to understand the thermomechanical mismatches between the materials and the adhesive joints exhibited high peel stresses at the overlap ends. The low weight content (2 and 5 wt.%) of Fe3O4 exhibited beneficial effects on the mechanical, thermal, thermomechanical, wettability and lap shear strength.

Acknowledgement

CH thanks Nanyang Technological University for the financial support in the form a SINGA graduate scholarship. IS thanks National Research Foundation Singapore for financial support via Grant Number CRP29-2022-0041.

Disclosure statement

No potential conflict of interest was reported by the author(s).

Nomenclature

A=

adhesive failure

Al=

aluminum

BET=

Brunauer – Emmett–Teller

CDCB=

contoured double-cantilever beam

CTE=

coefficient of thermal expansion

DMA=

dynamic mechanical analyzer

E=

Young’s modulus

EoLV=

end-of-life vehicles

εy=

failure strain in the y direction

FRP=

fiber reinforced polymers

GIC=

adhesive fracture energy

M=

mixed failure

Ra,1=

arithmetic mean height in the axial direction

Sa=

arithmetic mean height

Sp=

maximum height of peaks

Sssk=

skewness

Sz=

maximum height of the surface

SLJ=

single lap joint

σUTS=

Ultimate tensile strength

tan δ=

tan delta

Tg=

glass transition temperature

GIC=

thermal diffusivity

Al2O3=

aluminum oxide

C=

cohesive failure

CFRP=

carbon fiber reinforced polymers

DIC=

digital image correlation

DSC=

differential scanning calorimetry

=

storage modulus

εx=

failure strain in the x direction

Fe3O4=

iron oxide

GFRP=

glass fiber reinforced polymer

h=

height

P=

applied load

Ra,2=

arithmetic mean height in the transverse direction

Sku=

kurtosis

Sq=

root mean square height

Sv=

maximum height of valleys

SBT=

Simple Beam Theory

σfail=

failure strength

σYield=

yield strength

TEPs=

thermally expandable particles

TMA=

thermo-mechanical analyzer

Supplementary material

Supplemental data for this article can be accessed online at https://doi.org/10.1080/00218464.2023.2256670

Additional information

Funding

This work was supported by the National Research Foundation [CRP29-2022-0041].

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