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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 53, 2023 - Issue 20
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Articles

Palladium-copper catalyzed decarboxylation/de-cycloalkanonylative coupling reaction to synthesize 9,9-diaryl-xanthenes

Yongjun Zhanga Shandong Provincial Key Laboratory of Chemical Energy Storage and Novel Cell Technology, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong, ChinaView further author information
,
Zeyou Wangb State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian, Liaoning, ChinaView further author information
,
Shan Zhanga Shandong Provincial Key Laboratory of Chemical Energy Storage and Novel Cell Technology, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong, ChinaView further author information
,
Lijun Wanga Shandong Provincial Key Laboratory of Chemical Energy Storage and Novel Cell Technology, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong, ChinaView further author information
,
Zixuan Zhanga Shandong Provincial Key Laboratory of Chemical Energy Storage and Novel Cell Technology, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong, ChinaView further author information
,
Xiaoqing Zenga Shandong Provincial Key Laboratory of Chemical Energy Storage and Novel Cell Technology, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong, ChinaView further author information
,
Yalin Zhanga Shandong Provincial Key Laboratory of Chemical Energy Storage and Novel Cell Technology, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong, ChinaCorrespondence[email protected]
View further author information
&
Guodong Shena Shandong Provincial Key Laboratory of Chemical Energy Storage and Novel Cell Technology, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong, ChinaCorrespondence[email protected]
View further author information
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Pages 1751-1759 | Received 26 May 2023, Published online: 14 Aug 2023
 
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Abstract

An efficient palladium-copper catalyzed regioselective C–C bond cleavage/C–H bond activation/C–C bond reformation reaction to synthesize 9,9-diaryl-xanthenes has been developed. A variety of 9,9-diaryl-xanthenes were synthesized in moderate to good yields by 9H-xanthene-9-carboxylic acid/2-(9H-xanthen-9-yl)-cycloketones and aromatics bearing electron-donating functional groups through the decarboxylation/de-cycloalkanonylative coupling reactions.

Additional information

Funding

This work was financially supported by the Natural Science Foundation of Shandong Province (ZR2019QB022), the Doctoral Scientific Research Startup Foundation of Liaocheng University (No. 31805403) and the College Students’ Innovation and Entrepreneurship Training Program of Liaocheng University (CXCY2022190).

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