Effect of Y₂O₃ and TiO₂ addition of dispersed powder on phase evolution and microstructural analysis of (Al, Cu)₃Ti intermetallic synthesised via mechanical alloying and powder metallurgy route

ABSTRACT

Aluminium-based alloys are the most widely used structural material owing to their lightweight, high stiffness with moderate strength, ductility, and toughness. However, these alloys still have several issues in engineering applications, such as moderate strength, high temperature, wear-resistant, unstable mechanical characteristics, etc. Intermetallics offer tremendous possibilities for the development of advanced novel material with enhanced mechanical properties for aerospace and automotive applications due to the range of reinforcement materials and flexibility in their primary processing. The current research provides a detailed study of the formation of Cu₉Al₄, AlCu, and AlTi₃ intermetallic compounds via mechanical alloying and powder metallurgy route. The microstructural characterisation, compositional analysis, and evolution of different aluminium-based intermetallic compounds with respect to milling time were investigated through field emission scanning electron microscope (FESEM), energy-dispersive spectrometer (EDS), and X-ray diffraction (×RD) analysis. Microstructural analysis revealed that the elemental powder became fine and homogenous as the milling progressed. In addition, the grain structure is homogeneously distributed with a few enlarged and dispersed phases of Y₂O₃ and TiO₂ in the base alloy. The porosity of the sintered compacts was significantly improved by the addition of 1 wt % each of Y₂O₃ and TiO₂ dispersoids to 60 h milled base alloy.

KEYWORDS:

• Intermetallic
• milling parameters
• particle size
• microstructure
• powder metallurgy
• XRD
• SEM

Disclosure statement

No potential conflict of interest was reported by the author(s).