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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 2
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Original Articles

Dioxane Dibromide–Mediated Solvent‐Free Synthesis of Vicinal Dibromides

Subrata Kumar Chaudhuri Department of Chemistry, Organic Chemistry Section, Jadavpur University, Kolkata, India
,
Sanchita Roy Department of Chemistry, Organic Chemistry Section, Jadavpur University, Kolkata, India
,
Manabendra Saha Department of Chemistry, Organic Chemistry Section, Jadavpur University, Kolkata, India
&
Sanjay Bhar Department of Chemistry, Organic Chemistry Section, Jadavpur University, Kolkata, IndiaCorrespondence[email protected] [email protected]
Pages 271-274 | Received 01 Jun 2006, Published online: 25 Jul 2007
 
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Abstract

Structurally varied vicinal dibromides have been synthesized in high yield and good purity through highly stereoselective anti‐addition of bromine across the olefinic linkages using dioxane dibromide (DD) under solvent‐free conditions.

Acknowledgments

Financial support from the Council of Scientific and Industrial Research, Government of India (CSIR), New Delhi [Grant No. 01(1673)/00/EMR‐II] is gratefully acknowledged. S. R. thanks the University Grants Commission Government of India (UGC), New Delhi, and M. S. thanks CSIR, New Delhi, for Junior Research Fellowships. The authors express profound thanks to N. Dutta of the Indian Association for the Cultivation of Science (IACS) for necessary assistance.

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