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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 5
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Original Articles

One‐Pot Preparation of Fluorinated α‐Aminoalkyl Phosphonates under Microwave Irradiation and Solvent‐Free Conditions

Xiao‐yong Lv Department of Chemistry, School of Science, Shanghai University, Shanghai, China
,
Jian‐min Zhang Department of Chemistry, School of Science, Shanghai University, Shanghai, China
,
Chun‐hui Xing Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Science, Shanghai, China
,
Wei‐qiong Du Department of Chemistry, School of Science, Shanghai University, Shanghai, China
&
Shi‐zheng Zhu Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Science, Shanghai, ChinaCorrespondence[email protected]
Pages 743-757 | Received 03 Jul 2006, Published online: 10 Mar 2007
 
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Abstract

A facile one‐pot method has been developed for the synthesis of fluorine‐containing α‐amino phosphonates in good yields by a three‐component reaction of fluorinated aromatic aldehydes, anilines, and diethyl phosphate in the presence of a silica‐gel support under microwave irradiation within 10 min. All new compounds are fully characterized by spectral methods and elemental analysis.

Acknowledgments

This work was supported by the National Science Foundation of China (Nos. 20472106, 20532040).

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