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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 11
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Original Articles

Darzens Reaction Promoted by KF/Alumina: A Novel Stereoselective Method for Rapid and Efficient Synthesis of trans‐α,β‐Epoxy Ketones

Ali Sharifi Chemistry and Chemical Engineering Research Center of Iran, Tehran, IranCorrespondence[email protected]
,
Roghiyeh Salimi Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran
,
Mojtaba Mirzaei Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran
&
M. Saeed Abaee Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran
Pages 1825-1832 | Received 29 Jun 2006, Published online: 30 Jun 2007
 
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Abstract

The Darzens condensation of α‐chloroacetophenone with various aromatic aldehydes mediated by potassium fluoride on alumina at room temperature resulted in formation of good to excellent yields of trans‐α,β‐epoxy ketones in short time periods.

Acknowledgment

Partial financial support by the Ministry of Science, Research, and Technology of Iran is gratefully acknowledged.

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