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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 19
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Original Articles

Ce(SO4)2‐Mediated Nitration of N,N‐Dialkylanilines with NaNO2 in Water

Xianghua Yang Key Laboratory for Bioorganic Phosphorus Chemistry and Chemical Biology (Ministry of Education), Department of Chemistry, Tsinghua University, Beijing, China
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Chanjuan Xi Key Laboratory for Bioorganic Phosphorus Chemistry and Chemical Biology (Ministry of Education), Department of Chemistry, Tsinghua University, Beijing, ChinaCorrespondence[email protected]
Pages 3381-3392 | Received 12 Dec 2006, Published online: 05 Oct 2007
 
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Abstract

Ce(SO4)2‐mediated nitration of N,N‐dialkylanilines with NaNO2 using water as the solvent has been achieved in good to excellent yields. The nitrating reaction proceeded smoothly at ambient temperature.

Acknowledgments

This work was supported by the National Natural Science Foundation of China (20572058) and Beijing Department of Education (XK100030514).

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