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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 20
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Original Articles

Ferric Sulphate Hydrate–Catalyzed, Microwave‐Assisted Synthesis of 2,3‐Unsaturated O‐Glycosides via the Ferrier Reaction

Guisheng Zhang Henan Key Laboratory for Environmental Pollution Control, School of Chemical and Environmental Science, Henan Normal University, Xinxiang, Henan, ChinaCorrespondence[email protected]
&
Qingfeng Liu Henan Key Laboratory for Environmental Pollution Control, School of Chemical and Environmental Science, Henan Normal University, Xinxiang, Henan, China
Pages 3485-3492 | Received 26 Jan 2007, Published online: 05 Oct 2007
 
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Abstract

Fe2(SO4)3 · xH2O catalyzes the Ferrier reaction of per‐O‐acetylated/benzylated glycals with alcohols to give 2,3‐unsaturated α‐glycosides in a few minutes under microwave irradiation.

Acknowledgments

This work was supported by the Natural Science Foundation of China (No. 20672031) and the Program for New Century Excellent Talents in University of Henan Province.

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