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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 22
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Original Articles

Solvent-Free Synthesis of Nitrilotriacetamide and Diketopiperazines from Nitrilotriacetic Acid under Microwave Irradiation and Their Antimicrobial Activity

Gülşen Öztürk University of Dicle, Faculty of Science and Art, Department of Chemistry, Diyarbakır, TurkeyCorrespondence[email protected]
,
Bahattin Gümgüm University of Dicle, Faculty of Science and Art, Department of Chemistry, Diyarbakır, Turkey
,
Murat Kizil University of Dicle, Faculty of Science and Art, Department of Chemistry, Diyarbakır, Turkey
&
Sevil Emen University of Dicle, Faculty of Science and Art, Department of Chemistry, Diyarbakır, Turkey
Pages 3981-3988 | Received 01 Dec 2006, Published online: 19 Nov 2007
 
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Abstract

Efficient synthesis of dioxopiperazines‐diketopiperzines (DKPs)‐ and amide from nitrilotriacetic acid (NTA) using microwave irradiation and classical heating were described. All compounds were characterized using 1H NMR, 13C NMR and elemental analysis. Antimicrobial effects of these compounds are also investigated. All tested compounds showed moderate antimicrobial activity.

Acknowledgment

Financial support by University of Dicle (grant no: DÜAPK 04‐FF‐51) is gratefully acknowledged.

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