Erratum

In the article “New Route for the Syntheis of Pyrazole, Triazole, Triazine and Triazepine Derivatives” by Omran, Amer, and Khodairy, published in Synth. Commun. 36(24), 3647–3653, the following table was originally omitted. It was to be cited in the article on page 3648 at the end of the first paragraph.

Table 1.  Analytical and spectral data of the new compounds –

Product no.	M. P. (°C)^a	Yield (%)	Mole. form. (Mol.wt.)	Analytical data^b cal./found				IR (cm^−1)^c	^1H‐NMR ∂ (ppm)^d
				C	H	N	S
1	192–4	94	C19H23N3 (293.41)	77.78	7.90	14.32		3274, 3169 (2NH)	10.0 (s, 1H, NH), 8.0–7.1 (m, 10H, arom. +NH), 2.2–2.0[t, 4H, N (CH2)2], 1.4–1.0 (m, 6H, 3CH2)
				77.55	7.77	14.01
2 a	140–2	60	C21H22N6 (358.44)	70.37	6.19	23.45		3420, 3310 (NH2), 2192 (CN)	8.0–7.4 (m, 10H, arom.), 5.5–5.0 (br, 2H, NH2), 2.2–2.0[t, 4H, N (CH2)2], 1.0–1.4 (m, 6H, 3CH2)
				70.20	6.31	23.66
2 b	185–7	40	C20H23N5 (333.44)	72.04	6.95	21.00		3277, 3172 (NH2), 3050 (CHarom.)	8.0–7.3 (m, 10H, arom.), 6.2 (s, 1H, ˭CH), 5.5–5.2 (br, 2H, NH2), 2.3–2.0[t, 4H, N(CH2)2], 1.3–1.0 (m, 6H, 3CH2)
				72.31	6.72	21.26
3	211	29	C26H26N4 (394.52)	79.16	6.64	14.20		3049 (CHarom.), 1544 (C˭C)	8.0–7.0 (m, 18H, arom.), 6.0 (s, 1H, ˭CH), 2.3–2.0[t, 4H, N(CH2)2], 1.3–1.0 (m, 6H, 3CH2)
				79.32	6.78	14.35
4	320	60	C20H22N4O4 (334.42)	71.83	6.63	16.75		1717 (C˭O)	8.0–7.3 (m, 10H, arom.), 4.0 (s, 2H, CH2), 2.3–2.0[t, 4H, N(CH2)2], 1.3–1.0 (m, 6H, 3CH2)
				71.60	6.70	16.57
5 a	322	90	C21H24N6 (360.46)	69.97	6.71	23.31		3404, 3340, 3212 (NH, NH2), 2203 (CN)	9.0 (s, 1H, NH), 8.1–7.3 (m, 11H, arom. +NH), 5.5–5.2(br, 2H, NH2), 2.3–2.0[t, 4H, N(CH2)2], 1.3–1.0(m, 6H, 3CH2)
				69.71	6.85	23.57
5 b	216	70	C21H26N6O (378.48)	66.64	6.92	22.20		3440, 3414, 3220, 3211 (NH, NH2)	9.4 (s, 1H, NH), 8.0–7.1 (m, 11H, arom. +NH), 6.6–6.4 (br, 2H, NH2), 5.5–5.2 (br, 2H, NH2), 2.3–2.0[t, 4H, N(CH2)2], 1.3–1.0 (m, 6H, 3CH2)
				66.51	6.71	22.37
6	255	55	C23H28N4O3 (408.5)	67.63	6.91	13.72		3415 (OH), 3264 (NH), 1722 (C˭O)	9.2 (s, 2H, 2NH), 8.0–7.0 (m, 15H, arom.), 4.4 (s, 1H, OH), 4.1–3.8 (q, 2H, CH2), 2.3–2.0[t, 4H, N(CH2)2], 1.3–1.0 (m, 9H, 3CH2 +CH3)
				67.76	6.73	13.60
7 a	299	69	C25H25ClN4 (416.95)	72.02	6.04	13.44		3050 (CHarom.), 2927, 2860 (CHalip)	7.6–7.0 (m, 14H, arom.), 4.2 (s, 1H, CH), 2.4–2.1[t, 4H, N(CH2)2], 1.4–1.1 (m, 6H, 3CH2)
				72.39	6.23	13.59
7 b	210–2	80	C26H27N5O2 (441.53)	70.73	6.16	15.86		3059 (CHarom.), 2925, 2863 (CHalip)	7.6–7.0 (m, 14H, arom.), 2.4–2.1 [t, 4H, N(CH2)2], 1.4–1.1 (m, 9H, 3CH2+CH3)
				70.50	6.30	15.70
8	188	30	C19H20N4S (336.45)	67.83	5.99	16.65	9.53	3052 (CHarom.), 1150 (C˭S)	7.6–7.0 (m, 10H, arom.), 2.4–2.1 [t, 4H, N(CH2)2], 1.4–1.1 (m, 6H, 3CH2)
				67.98	5.80	16.82	9.70
9 a	223	75	C25H27N5O (413.52)	72.61	6.58	16.94		3389 (OH), 3200, 3223 (2NH), 1676 (C˭O)	9.0 (s, 1H, NH), 8.0–7.0 (m, 15H, arom.), 6.0 (s, 1H, OH), 2.3–2.0 [t, 4H, N(CH2)2], 1.3–1.0 (m, 6H, 3CH2)
				72.54	6.77	16.8
9 b	187	77	C25H27N5S (429.58)	69.9	6.33	16.3	7.46	3281,3176(2NH), 1102(C˭S)	9.2 (s, 2H, 2NH), 8.0–7.0 (m, 15H, arom.), 2.3–2.0 [t, 4H, N(CH2)2], 1.3–1.0 (m, 6H, 3CH2)
				69.76	6.40	16.5	7.66
10	250–2	80	C25H27N5 (395.51)	75.92	6.37	17.71		3051 (CHarom.), 1553 (C˭N)	7.6–7.0 (m, 15H, arom.), 2.4–2.1 [t, 4H, N(CH2)2], 1.4–1.1 (m, 6H, 3CH2)
				75.77	6.56	17.90
11	215	93	C25H27N4OPS (415.49)	64.96	5.88	12.11	6.93	2927 (CHalip.), 1110 (P˭S)	7.6–7.0 (m, 14H, arom.), 3.5 (s,3H, OCH3), 2.4–2.1 [t, 4H, N(CH2)2], 1.4–1.1 (m, 6H, 3CH2)
				64.76	5.66	12.32	6.81
12	176	77	C23H23N5OS (417.53)	66.16	5.55	16.77	7.68	2196 (CN), 690 (C‐S‐C)	8.0–7.6 (m, 10H, arom.), 2.8 (s, 3H, SCH3), 2.4–2.1 [t, 4H, N(CH2)2], 1.4–1.1 (m, 6H, 3CH2)
				66.32	5.66	16.60	7.90
13	112–4	70	C28H26N6 (446.57)	75.31	5.87	18.82		3234 (NH), 2193 (CN)	10.0 (s, 1H, NH), 8.0–7.4 (m, 15H, arom.), 2.4–2.1 [t, 4H, N(CH2)2], 1.4–1.1 (m, 6H, 3CH2)
				75.5	5.69	18.90
14	169	66	C28H25N5O (447.54)	75.15	5.63	15.65		2212 (CN), 1696 (C˭O)	8.1–7.3 (m, 15H, arom.), 2.4–2.1 [t, 4H, N(CH2)2], 1.4–1.1 (m, 6H, 3CH2)
				75.33	5.89	15.89
^aUncorrected.
^bSatisfactory microanalysis obtained C;±0.35, H; ±0.40, N; ±0.30.
^cMeasured by Nicolet FT‐IR 710 spectrophotometer.
^dMeasured by a Varian EM 360 L spectrometer at 60 MHz using TMS as internal standard and DMSO as a solvent.

The publisher wishes to express its sincere regret for this omission.