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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 9
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Original Articles

Uncatalyzed Hydrogen-Transfer Reductions of Aryl Ketones

S. Srinivasan Department of Industrial Chemistry, Alagappa University, Karaikudi, India
&
P. Manisankar Department of Industrial Chemistry, Alagappa University, Karaikudi, IndiaCorrespondence[email protected]
Pages 1338-1347 | Received 13 Dec 2009, Published online: 30 Mar 2011
 
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Abstract

A simple, convenient, and environmentally benign procedure has been developed for exclusive reduction of aryl ketones by hydrogen transfer with sec-BuOH as hydrogen donor in the presence of KOH without supercritical conditions, ligands, and any catalytic utility.

Notes

a Isolated yield after purification by column chromatography.

b Unreacted ketone almost recovered.

c Multiple spots observed on TLC.

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