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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 15
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Original Articles

Preparation of Amidines from Amidoximes via Transfer Hydrogenation

Umesh S. Mahajan Department of Chemistry, Mahatma Phoole, ASC College, Panvel, Raigad, India
,
Rupesh R. Godinde Department of Chemistry, Mahatma Phoole, ASC College, Panvel, Raigad, India
&
P. N. Mandhare Department of Chemistry, Mahatma Phoole, ASC College, Panvel, Raigad, IndiaCorrespondence[email protected]
Pages 2195-2199 | Received 28 Sep 2009, Published online: 25 May 2011
 
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Abstract

Amidoximes are reduced into amidine using triethyl silane and PdCl2 in acetic acid.

ACKNOWLEDGMENT

The authors thank Dr. Dhanjay Sathe, associate vice president of USV Limited, for valuable suggestions.

Notes

Note. Isolated yield: all products were characterized by NMR (1H and 13C).

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