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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 42, 2012 - Issue 7
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Original Articles

Environmentally Benign One-Pot Synthesis of Cyanamides from Dithiocarbamates Using I2 and H2O2

Latonglila Jamir Department of Chemistry, Nagaland University, Lumami Campus, Nagaland, India
,
Upasana Bora Sinha Department of Chemistry, Nagaland University, Lumami Campus, Nagaland, IndiaCorrespondence[email protected]
,
Jayashree Nath Centre for the Environment, Indian Institute of Technology Guwahati, Guwahati, Assam, India
&
Bhisma K. Patel Department of Chemistry, Indian Institute of Technology Guwahati, Guwahati, Assam, India
Pages 951-958 | Received 01 Jun 2010, Published online: 16 Dec 2011
 
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Abstract

An environmentally benign reaction is devised for the synthesis of cyanamides from dithiocarbamate salts using iodine and H2O2.

GRAPHICAL ABSTRACT

ACKNOWLEDGMENTS

B. K. P. acknowledges the support from the Department of Science and Technology, New Delhi (SR/S1/OC-15/2006), and the Council of Scientific and Industrial Research (CSIR) [01(2270)/08/EMR-II]. L. J. thanks the CSIR for fellowship. Thanks are also given to CIF, Indian Institute of Technology, Guwahati for NMR spectra.

Notes

a Reactions were monitored by TLC.

b Confirmed by IR, 1H NMR, and 13C NMR.

c Isolated yield.

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