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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 51, 2021 - Issue 1
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Articles

Rh(III)−catalyzed synthesis of isoquinolines from N-hydroxyoximes and alkynes in γ-valerolactone

Kuan-Chang Jianga School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, ChinaView further author information
,
Liang Wanga School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, China;b School of Chemical and Pharmaceutical Engineering, Changzhou Vocational Institute of Engineering, Changzhou, ChinaCorrespondence[email protected]
View further author information
,
Qun Chena School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, ChinaView further author information
,
Ming-Yang Hea School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, ChinaView further author information
,
Ming-Gui Shenc National Engineering Laboratory for Biomass Chemical Utilization, Key and Open Laboratory on Forest Chemical Engineering, Key Laboratory of Biomass Energy and Material, Institute of Chemical Industry of Forest Products, Nanjing, ChinaView further author information
&
Zhi-Hui Zhanga School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, ChinaCorrespondence[email protected]
View further author information
Pages 94-102 | Received 23 Jun 2020, Published online: 14 Sep 2020
 
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Abstract

A Rh (III)−catalyzed synthesis of isoquinoline derivatives from N-hydroxyoximes and alkynes via C–H activation/annulation process in biomass-derived γ-valerolactone (GVL) has been developed. A series of functional groups were well tolerated, affording the desired products in good to excellent yields.

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Additional information

Funding

We gratefully acknowledge the China Postdoctoral Science Foundation [2018M632289], the Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology [BM2012110], the Priority Academic Program Development (PAPD) of Jiangsu Higher Education Institutions, and Jiangsu Key Laboratory of Biomass Energy and Material [JSBEM201806] for the financial support.

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