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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 51, 2021 - Issue 17
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Articles

Synthesis of 1,2-diketones by mercury-catalyzed alkyne oxidation

Xiaochuan MeiCollege of Biological and Environmental Sciences, Zhejiang Wanli University, Ningbo, PR ChinaView further author information
,
Weican HuCollege of Biological and Environmental Sciences, Zhejiang Wanli University, Ningbo, PR ChinaView further author information
,
Kexin GaoCollege of Biological and Environmental Sciences, Zhejiang Wanli University, Ningbo, PR ChinaView further author information
,
Haotian GaoCollege of Biological and Environmental Sciences, Zhejiang Wanli University, Ningbo, PR ChinaView further author information
,
Chaoyang WangCollege of Biological and Environmental Sciences, Zhejiang Wanli University, Ningbo, PR ChinaView further author information
,
Guoying QianCollege of Biological and Environmental Sciences, Zhejiang Wanli University, Ningbo, PR ChinaCorrespondence[email protected]
View further author information
&
Zhouting RongCollege of Biological and Environmental Sciences, Zhejiang Wanli University, Ningbo, PR ChinaCorrespondence[email protected]
ORCID Iconhttps://orcid.org/0000-0001-7811-4890View further author information
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Pages 2661-2667 | Received 18 Apr 2021, Published online: 30 Jun 2021
 
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Abstract

The first mercury-catalyzed synthesis of 1,2-diketones by alkyne oxidation has been developed. This inexpensive method extends the potential of mercury catalysis and allows the rapid construction of various 1,2-diketones and α-carbonyl amides in good yields with high functional group tolerance.

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Additional information

Funding

This work was supported by the Natural Science Foundation of Zhejiang Province [LQ21B020010], Scientific Research Fund of Zhejiang Provincial Education Department [Y201942345], the Natural Science Foundation of Ningbo [2019A610193], the Zhejiang Provincial Top Key Discipline of Bioengineering [ZS2017014].

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