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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 51, 2021 - Issue 22
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Articles

Cu(OTf)2-Catalyzed efficient sulfonylation of vinyl azides with sodium sulfinates

Zhitao NingCollege of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou, ChinaView further author information
,
Zheng XuCollege of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou, ChinaView further author information
,
Ruikai LiuCollege of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou, ChinaView further author information
&
Zhengyin DuCollege of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou, ChinaCorrespondence[email protected]
View further author information
Pages 3492-3500 | Received 02 Jun 2021, Published online: 11 Oct 2021
 
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Abstract

A simple oxidative cross-coupling reaction between vinyl azides and sodium sulfinates was developed. This reaction uses commercial arylsulfinates that are more efficient, cheaper, and more stable as sulfonylation reagents, for efficiently, cheaply, and environmentally friendly synthesis of β-keto sulfones. And the reaction has the advantages of simple operation, high efficiency, good yield, and also has a wide range of functional group tolerance.

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Funding

Financial supports by the National Natural Science Foundation of China (Nos. 21262028, 21762039) and the Natural Science Foundation of Gansu Province (No. 20JR5RA521) are acknowledged.

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