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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 1
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Original Articles

THE SYNTHESIS AND STRUCTURE CHARACTERISTICS OF TWO NOVEL AZO-QUINONE DERIVATIVES

Li Hai-ying Petrochemical Department, Fushun Petroleum Institute, Fushun, 113001, China
&
Lei Liang-cai Petrochemical Department, Fushun Petroleum Institute, Fushun, 113001, China
Pages 155-158 | Received 02 Apr 2000, Published online: 09 Nov 2006
 
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Abstract

The synthesis of novel LB film materials 2-(4-hexadecyloxyphenylazo)anthraquinone and 2-(4-dodecyloxyphenylazo) anthraquinone is described. These materials were obtained from 2-amino-anthraquinone by azo-coupling with phenol and follwed by Williamson etherification of phenolic hydroxyl group with alkyl bromide. The structures were confirmed by NMR, MS, FT-IR techniques and elemental analysis.

Acknowledgments

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