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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 3
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Original Articles

THE HIGH STEREOSELECTIVE SYNTHESIS OF β-ALKYNYL-ENOL PHOSPHATES

Yixiang Ding Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 354 Fenglin Road, Shanghai, 200032, People's Republic of China
&
Xiaogen Huang Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 354 Fenglin Road, Shanghai, 200032, People's Republic of China
Pages 449-454 | Received 21 Mar 2000, Published online: 09 Nov 2006
 
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Abstract

A high stereoselective synthesis for β-alkynyl-enol phosphates from β-alkynyl ketone and dialkyl phosphite, via Atherton--Todd reaction, was reported. NaH as base gave a nearly pure Z-isomer.

ACKNOWLEDGMENT

The project was supported by the National Science Foundation of China.

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