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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 3
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Original Articles

CONVENIENT SYNTHESIS OF (R)-1,3-NONANEDIOL

Jozef Kula Institute of General Food Chemistry, Technical University of Lodz, Lodz, 90-924, Poland
,
Thuat Bui Quang Institute of General Food Chemistry, Technical University of Lodz, Lodz, 90-924, Poland
&
Krzysztof Smigielski Institute of General Food Chemistry, Technical University of Lodz, Lodz, 90-924, Poland
Pages 463-467 | Published online: 09 Nov 2006
 
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Abstract

Ozonolysis of methyl ricinoleate in methanol followed by an electrochemical reduction of the intermediate hydroperoxides on a Pb-cathode gave (R)-(−)-1,3-nonanediol with 65% yield. The diol was successfully used for optical resolution of racemic menthone.

ACKNOWLEDGMENT

This work was supported in part by research grant from KBN (3T09 B03012).

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