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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 6
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Original Articles

ALUMINA-SUPPORTED SYNTHESIS OF THIADIAZOLYL THIAZOLOTHIONES

M. Kidwai Department of Chemistry, University of Delhi, Delhi, 110007, India
,
P. Misra Department of Chemistry, University of Delhi, Delhi, 110007, India
&
K. R. Bhushan Department of Chemistry, University of Delhi, Delhi, 110007, India
Pages 817-822 | Received 13 Mar 2000, Published online: 09 Nov 2006
 
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Abstract

The expeditious solventless synthesis of 3-[5′-alkyl-1′3′4-thiadiazol-2-yl]-4-phenyl/hydroxy-2-thiazolothiones is described from readily accessible 2-amino-5-alkyl-1,3,4-thiadiazoles on basic alumina that are accelerated by exposure to microwaves.

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