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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 19
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Original Articles

AN IMPROVED METHOD FOR SYNTHESIS OF JACOBSEN'S CATALYST

Ivica Cepanec Belupo Ltd. Pharmaceuticals and Cosmetics, Radnička c. 224, Zagreb, HR-10000, Croatia
,
Hrvoje Mikuldaš Belupo Ltd. Pharmaceuticals and Cosmetics, Radnička c. 224, Zagreb, HR-10000, Croatia
&
Vladimir Vinković Ruđer Bošković Institute, Bijenička c. 54, Zagreb, HR-10002, CroatiaCorrespondence[email protected]
Pages 2913-2919 | Received 26 Jun 2000, Published online: 16 Aug 2006
 
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Abstract

The improved synthesis of Jacobsen catalyst 1 was developed. For both enantiomers the obtained overall yield starting from commercially available 4 was 80–85%.

ACKNOWLEDGMENT

The authors wish to express their gratitude to the Belupo Ltd. Pharmaceuticals and Cosmetics for the financial support of this research.

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