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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 22
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Original Articles

1,4-PENTADIEN-3-ONES. A SOURCE FOR SELENANO 1,2,3- SELENA AND THIADIAZOLES

D. Bhaskar Reddy Department of Chemistry, Sri Venkateswara University, Tirupati, 517 502, India
,
A. Somasekhar Reddy Department of Chemistry, Sri Venkateswara University, Tirupati, 517 502, India
&
V. Padmavathi Department of Chemistry, Sri Venkateswara University, Tirupati, 517 502, India
Pages 3429-3437 | Received 01 Sep 1999, Published online: 22 Aug 2006
 
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Abstract

The 4-Selenanols (2,3) and 4-selenanones (4) were obtained by the reaction of 1,4-pentadien-3-ones (1) with sodium hydrogen selenide under different conditions. The fused 1,2,3-selenadiazoles (6) and 1,2,3-thiadiazoles (7) were prepared from 4 on oxidative cyclization with SeO2 and Hurd–Mori reaction with SOCl2.

ACKNOWLEDGMENT

We acknowledge the University Grants Commission, New Delhi for providing Major Research Project to Prof. D. B. R. and V. P and Dr. Reddy's Research Foundation, Hyderabad for running NMR and Mass spectra.

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