Abstract
A new regioselective 2-O-deacetylation methodology of acetylated glycosides using 85% hydrazine hydrate in THF is described. Using this method, acetylated 1-thio-glycoside could also be selectively deprotected to give 3-O-deprotected compound.
Acknowledgments
The work was supported by The National Natural Science Foundation of China (No. 20272051) and by The Teaching and Research Award Program for Outstanding Young Teachers in Higher Education Institutions of MOE, P.R.C.